Synthesis of zearalenone-16-β,D-glucoside and zearalenone-16-sulfate: A tale of protecting resorcylic acid lactones for regiocontrolled conjugation.

H, Mikula; J, Weber; D, Svatunek; P, Skrinjar; G, Adam; R, Krska; C, Hametner; J, Fröhlich

doi:10.3762/bjoc.10.112

Public

Synthesis of zearalenone-16-β,D-glucoside and zearalenone-16-sulfate: A tale of protecting resorcylic acid lactones for regiocontrolled conjugation.

Shared by NobleBlocks on May 15, 2014 • 12:00 AM UTC

Authors:

Mikula H

Weber J

Svatunek D

Abstract

The development of a reliable procedure for the synthesis of the 16-glucoside and 16-sulfate of the resorcylic acid lactone (RAL) type compound zearalenone is presented. Different protective group strategies were considered and applied to enable the preparation of glucosides and sulfates that are di...

Subject

Sulfation

Glycosylation

Zearalenone

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