Reaction of Butyltin Hydroxide Oxide with p-Toluenesulfonic Acid: Synthesis, X-ray Crystal Analysis, and Multinuclear NMR Characterization of {(BuSn)12O14(OH)6}(4-CH3C6H4SO3)2

Eychenne‐Baron, Christophe; Ribot, François; Steunou, Nathalie; Sánchez, Clément; Fayon, Franck; Biesemans, Monique; C. Martins, José; Willem, Rudolph

doi:10.1021/om990877a

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Reaction of Butyltin Hydroxide Oxide with p-Toluenesulfonic Acid: Synthesis, X-ray Crystal Analysis, and Multinuclear NMR Characterization of {(BuSn)12O14(OH)6}(4-CH3C6H4SO3)2

Published in Organometallics • Apr 14, 2000

Authors:

Christophe Eychenne‐Baron

François Ribot

Nathalie Steunou

Abstract

The reaction of butyltin hydroxide oxide, BuSnO(OH), with p -toluenesulfonic acid, 4-CH 3 C 6 H 4 SO 3 H, yields the butyltin oxo cluster {(BuSn) 12 (μ 3 -O) 14 (μ 2 -OH) 6 } 2+ mixed with a soluble ill-defined butyltin oxo polymer, the presence of which was established by solid-state and quantitati...

Subject

Chemistry

Crystal structure

NMR spectra database

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