XAFS, IR, and UV−vis (diffuse reflectance and photoluminescence) spectroscopies have been employed to investigate the local environment of Cu I in Cu I -ZSM-5 prepared by gas phase reaction of H-ZSM-5 (SiO 2 /Al 2 O 3 = 90−50) with CuCl. The measurements confirm that the absolutely predominant coppe...
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