Very Fast Two-Dimensional NMR Spectroscopy for Real-Time Investigation of Dynamic Events in Proteins on the Time Scale of Seconds

Schanda, Paul; Brutscher, Bernhard

doi:10.1021/ja051306e

Public

Very Fast Two-Dimensional NMR Spectroscopy for Real-Time Investigation of Dynamic Events in Proteins on the Time Scale of Seconds

Published in Journal of the American Chemical Society • May 14, 2005

Authors:

Paul Schanda

Bernhard Brutscher

Abstract

We demonstrate for different protein samples that 2D 1H-15N correlation NMR spectra can be recorded in a few seconds of acquisition time using a new band-selective optimized flip-angle short-transient heteronuclear multiple quantum coherence experiment. This has enabled us to measure fast hydrogen-d...

Subject

Chemistry

Heteronuclear molecule

Deuterium NMR

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