Semiautomated High-Throughput Extraction and Cleanup Method for the Measurement of Polybrominated Diphenyl Ethers, Polybrominated Biphenyls, and Polychlorinated Biphenyls in Human Serum

Sjödin, Andreas; S. Jones, Richard; R. Lapeza, Chester; Focant, Jean-François; McGahee, Ernest; G. Patterson, Donald

doi:10.1021/ac030381+

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Semiautomated High-Throughput Extraction and Cleanup Method for the Measurement of Polybrominated Diphenyl Ethers, Polybrominated Biphenyls, and Polychlorinated Biphenyls in Human Serum

Published in Analytical Chemistry • Feb 24, 2004

Authors:

Andreas Sjödin

Richard S. Jones

Chester R. Lapeza

Abstract

A semiautomated extraction and cleanup method has been developed for the measurement of eight polybrominated diphenyl ethers (PBDEs), 2,2',4,4',5,5'-hexabromobiphenyl (BB-153) and 2,2',4,4',5,5'-hexachlorobiphenyl (CB-153). The method employs automated addition of internal standards ((13)C-labeled),...

Subject

Chemistry

Polybrominated diphenyl ethers

Chromatography

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