Synthesis of metal–organic frameworks by continuous flow

A. Bayliss, Peter; A. Ibarra, Ilich; Pérez, Eduardo; Yang⧫, Sihai; C. Tang, Chiu; Poliakoff, Martyn; Schröder, Martin

doi:10.1039/c4gc00313f

Public

Synthesis of metal–organic frameworks by continuous flow

Published in Green Chemistry • Jan 1, 2014

Authors:

Peter A. Bayliss

Ilich A. Ibarra

Eduardo Pérez

Abstract

MIL-53(Al) can be prepared via reaction in continuous flow in only 5–6 minutes with a space time yield of 1300 kg m−3 d−1. Extraction of free terephthalic acid from within the pores of MIL-53(Al) using supercritical ethanol has been developed.

Subject

Terephthalic acid

Continuous flow

Supercritical fluid

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