Abstract Herein, mesoporous V 2‐x Sb 2x O 5‐δ (Sb−V−O) compounds, encompassing a compositional range of x varying between, 0.05≤x≤0.08, with orthorhombic Pmmn space group symmetry, are synthesized by high‐temperature solid‐state reaction method. Scanning electron microscopy indicated the formation o...
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