Abstract Nickel-incorporated vanadium pentoxide (V 2-2x Ni 3x O 5-δ , 0.03 ≤ x ≤ 0.06) microparticles were synthesized and structurally characterized, revealing a biphasic composition dominated by orthorhombic V 2 O 5 with Pmmn space group and a minor triclinic NiV 2 O 6 phase with cap P 1 ̅ $P̅{1}$...
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